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• W2063011627 abstract "Today it is common to find samples with various additives from several families. This is the case of sweeteners, preservatives and antioxidants. We have selected a set of additives broadly used in foods and cosmetics with an ample variety of polarities, namely: aspartame (AS), acesulfame (AK)/saccharin (SA), methylparaben (MP), ethylparaben (EP), propylparaben (PP), butylparaben (BP), propylgallate (PG) and butylhydroxyanisole (BA). The monolithic column used as separative system is a 5 mm commercial precolumn of silica C18 coupled to a flow injection manifold working with a peristaltic pump. The mixture was separated in only 400 s with resolution factors greater than 1.1 in all cases. To achieve the separation in the FIA system we used two carriers: first, a mixture of ACN/water buffered with 10 mM pH 6.0 phosphate buffer and second, a methanol:water mixture to improve the carrier strength and speed up the more apolar analytes at 3.5 mL min(-1). Detection is accomplished by means of a diode array spectrometer at the respective wavelength of each compound. The comparison of the analytical parameters obtained for this procedure with a standard HPLC method validates our new method, obtaining a method that is quick, with high repeatability and reproducibility and with good resolution between analytes. We have successfully applied the method to real food and cosmetics samples." @default.
• W2063011627 created "2016-06-24" @default.
• W2063011627 creator A5031732697 @default.
• W2063011627 creator A5067050567 @default.
• W2063011627 creator A5089600698 @default.
• W2063011627 date "2007-07-01" @default.
• W2063011627 modified "2023-10-13" @default.
• W2063011627 title "Simultaneous determination of antioxidants, preservatives and sweetener additives in food and cosmetics by flow injection analysis coupled to a monolithic column" @default.
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• W2063011627 doi "https://doi.org/10.1016/j.aca.2007.05.040" @default.
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