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• W2063103542 abstract "The nitriding by plasma has the potential to improve the tribological and mechanical properties on a number of substrates, and offers various advantages as compared with other methods used in the modification of surfaces. We prepared four samples by nitriding the iron substrates in a gas mixture (80% H2 and 20% N2) under a pressure of 9.0 mbar, discharge frequency of 10 kHz and temperature of 773 K, for periods of 1, 2, 4 and 6 h. We characterised the samples by scanning electron microscopy (SEM), X-ray diffraction (XRD) and microhardness techniques, and detected the presence of Fe4N and Fe2–3N phases. We employed X-ray photoelectron spectroscopy (XPS) to obtain chemical-state and quantitative information of the plasma-nitrided iron surfaces. In situ cleaning was carried out by argon ion bombardment. The Fe 2p3/2 photoelectron peaks for all samples presented three components, associated with Fe0, Fe2+ and Fe3+, while the N 1s lines showed two components, the main one due to iron nitride and the other is connected with oxidised nitrogen." @default.
• W2063103542 created "2016-06-24" @default.
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• W2063103542 date "1999-04-01" @default.
• W2063103542 modified "2023-10-12" @default.
• W2063103542 title "Surface characterisation of plasma-nitrided iron by X-ray photoelectron spectroscopy" @default.
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• W2063103542 doi "https://doi.org/10.1016/s0169-4332(98)00809-5" @default.
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