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- W2063152199 abstract "Abstract This work describes the determination of mancozeb in insecticide samples using batch injection analysis (BIA) with pulsed amperometric detection (PAD) on boron-doped diamond (BDD) electrodes. The BIA amperometric parameters were evaluated and the best responses were achieved in phosphate solution at pH 9.0, using a detection potential of 0.3 V, cleaning potential of 0.0 V, dispensing rate of 160 μL s −1 and injection volume of 100 μL. A linear analytical curve was observed in the 40–650 μmol L −1 range, with a detection limit of 5.1 4 × 10 −7 mol L −1 . The determination of mancozeb in the insecticide samples proved to be in agreement with the standard iodometric titration (CIPAC method), with a 95% confidence level and with a relative error lower than 2%. In this way, the BIA–PAD method presented a fast response, high sensitivity, good repeatability and good reproducibility." @default.
- W2063152199 created "2016-06-24" @default.
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- W2063152199 date "2014-11-01" @default.
- W2063152199 modified "2023-10-14" @default.
- W2063152199 title "Fast and direct determination of mancozeb through batch injection analysis with amperometric detection on boron-doped diamond electrodes" @default.
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- W2063152199 doi "https://doi.org/10.1016/j.jelechem.2014.09.025" @default.
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