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- W2063415002 abstract "6-[3-(1-Adamantyl)-4-methoxyphenyl]-2-naphthoic acid (1), a promising new compound for the treatment of disorders of keratinization, has been synthesized in [14C]-labelled form from barium [14C]-carbonate via labelled benzene. Benzene-[U-14C] was converted to 4-bromo-methoxybenzene-[phenyl-U-14C] in six steps. Introduction of the adamantyl ring was carried out using 1-acetoxyadamantane under acid catalysis. 2-(1-Adamantyl)-4-bromo-methoxybenzene-[phenyl-U-14C] (2) was converted to a zincate and coupled with methyl 6-bromo-2-naphthoate using a nickel catalyst. The product of the aryl coupling reaction (3) was then saponified to give 6-[3-(1-adamantyl)-4-methoxyphenyl-[phenyl-U-14C]]-2-naphthoic acid." @default.
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- W2063415002 date "1991-07-01" @default.
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- W2063415002 title "Synthesis of carbon-14 labelled CD 271 (6-[3-(1-adamantyl)-4-methoxyphenyl]-2-naphthoic acid) a potential new agent for dermatology" @default.
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- W2063415002 doi "https://doi.org/10.1002/jlcr.2580290715" @default.
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