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• W2063513477 endingPage "4428" @default.
• W2063513477 startingPage "4399" @default.
• W2063513477 abstract "We describe a convenient, chemoselective asymmetric reductive amination procedure for the conversion of ketones to chiral hydrazines and amines. The key step in the three-step process is enantioselective DuPHOS-Rh-catalyzed hydrogenation of the CN double bond of N-acylhydrazones. Detailed optimization studies revealed the effect of solvent, temperature, and the N-acyl group on the enantioselectivity and catalytic efficiency of the reaction. The reduction products, N-acylhydrazines, were converted to hydrazines or amines through hydrolysis or treatment with samarium(II) iodide, respectively." @default.
• W2063513477 created "2016-06-24" @default.
• W2063513477 creator A5046240576 @default.
• W2063513477 creator A5059131009 @default.
• W2063513477 creator A5066501030 @default.
• W2063513477 creator A5069664761 @default.
• W2063513477 date "1994-04-01" @default.
• W2063513477 modified "2023-10-18" @default.
• W2063513477 title "Catalytic asymmetric reductive amination of ketones via highly enantioselective hydrogenation of the CN double bond" @default.
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