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- W2064047406 abstract "Two synthetic routes lead to [14C] LF.1695. The first one starts with labelled triphenyl methyl phosphonium iodide. This Wittig reagent reacts with benzyl piperidinone to afford benzylmethylidene piperidine 3. The reduction of 3 gives labelled pipecoline 4 which is condensed with an adduct affording an intermediate nitro compound 5. LF.1695 6 labelled at the methyl group is then obtained by catalytic reduction. The second route uses labelled chloro-nitro benzoic acid as starting material. The treatment of the corresponding acid chloride by Friedel-Crafts reaction gives the chloro-nitro-chloro-benzophenone 9 in good yield. Condensation of 9 with pipecoline according to the method described above gives an intermediate nitro compound 10 which is reduced to afford LF.1695 11 labelled at the carbonyl group." @default.
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- W2064047406 date "1984-10-01" @default.
- W2064047406 modified "2023-09-25" @default.
- W2064047406 title "Synthesis of [14C]2-pipecolinyl-5-amino-4′-chloro-benzophenone (LF.1695)" @default.
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- W2064047406 doi "https://doi.org/10.1002/jlcr.2580211003" @default.
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