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- W2064248735 abstract "Decomplexation of Ca3(thd)6 by mono- and bidentate N-donors [morpholine, dimorpholinoethane (DIMOE), TMEDA, bipyridine] afforded the corresponding adducts Ca(thd)2L [L=morpholine (1a), DIMOE (1b), TMEDA (2)] and {Ca(thd)2}2(bipy) (3). All complexes have been fully characterised by elemental analysis, FT-IR and 1H NMR spectroscopy. Compounds 1b and 3 have also been characterised by X-ray crystallography. The structure of 3 is based on six- and seven-coordinated Ca centres; it is the first dimeric volatile Lewis base adduct of Ca(thd)2. The thermal behaviour of all derivatives has been studied by thermal gravimetric analysis." @default.
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- W2064248735 date "2001-04-01" @default.
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- W2064248735 title "Calcium tetramethylheptanedionate adducts with N-donor ligands. Molecular structure of a dimeric and volatile adduct Ca2(η2-thd)(μ,η2-thd)3(η2-bipy)" @default.
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- W2064248735 doi "https://doi.org/10.1016/s0277-5387(01)00756-2" @default.
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