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• W2064533623 abstract "[reaction: see text] A new method for the one-pot asymmetric reductive amination of prochiral aliphatic ketones has been developed. The previously unexplored reagent combination of Ti(O(i)Pr)(4)/Raney Ni/H(2) in the presence of (R)- or (S)-alpha-methylbenzylamine provides good to excellent yield (76-90%) and diastereomeric excess (72-98%). The second step, hydrogenolysis, provides the corresponding primary amine in high yield (88-93%) and with uncompromised enantiomeric excess." @default.
• W2064533623 created "2016-06-24" @default.
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• W2064533623 date "2005-10-01" @default.
• W2064533623 modified "2023-10-18" @default.
• W2064533623 title "Evolution of Titanium(IV) Alkoxides and Raney Nickel for Asymmetric Reductive Amination of Prochiral Aliphatic Ketones" @default.
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• W2064533623 doi "https://doi.org/10.1021/ol051909v" @default.
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