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- W2064565395 abstract "Abstract The development of a practical method for the preparation of vinylamino-β -lactams from Dane salts and Schiff bases is described. Among the reagents known to produce β-lactams from imines and acetic acids, only phenyl dichlorophosphate and 1-methyl-2-chloropyridinium iodide are suitable for the synthesis of vinylamino- β-lactams. Reaction of acetic acids with ethanolimine derivatives promoted by phenyl dichlorophosphate affords oxazolidines instead β-lactams. Protection of the hydroxyl group as the trimethylsilyl ether in the starting Schiff bases provides a convenient route to the corresponding β-lactams instead oxazolidines. Some observations on the scope of the method are made." @default.
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- W2064565395 date "1985-01-01" @default.
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- W2064565395 title "Syntheses of β-lactams from acetic acids and imines induced by phenyl dichlorophosphate reagent" @default.
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- W2064565395 doi "https://doi.org/10.1016/s0040-4020(01)96484-1" @default.
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