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- W2064578288 abstract "Abstract A method is described for the determination of 0.001–0.01% lead in high-alloy steels by atomic absorption spectroscopy following solvent extraction. After sample dissolution, the bulk of the iron is removed by extraction with diisopropyl ether and residual traces of iron(III) are reduced with hydroxylammonium chloride. Lead is extracted as tetraiodoplumbate into methyl isobutyl ketone and the organic extract is sprayed into the flame. Iodine, which is liberated during the iodide extraction, particularly in the presence of copper, inhibits the extraction of lead, and the copper which is extracted also produces slight interference. Both the effects can be standardised by the addition of 0.012 g of copper to the aqueous solution before the iodide extraction in both the steel samples and the lead solutions for calibration." @default.
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- W2064578288 modified "2023-09-26" @default.
- W2064578288 title "The determination of trace amounts of lead in high-alloy steels by solvent extraction and atomic absorption spectroscopy" @default.
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