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• W2064596567 endingPage "1734" @default.
• W2064596567 startingPage "1727" @default.
• W2064596567 abstract "The morphology and melting behaviour of ε-caprolactone-styrene diblock copolymers (PCL-b-PS) quenched from the melt were investigated by small-angle X-ray scattering and differential scanning calorimetry as a function of glass transition temperature of the PS block, Tg,PS. A plasticizer miscible only with the PS block, such as polystyrene oligomer or dioctyl phthalate, was added to PCL-b-PS in order to decrease Tg,PS successively (plasticizer-added PCL-b-PS). The crystallizability of the PCL block depended strongly on Tg,PS; the PCL block did not crystallize when Tg,PS was higher than the crystallization temperature Tc, while it crystallized partially when Tg,PS was lower than Tc. However, details of the morphology formed (i.e. the long spacing and lamellar thickness) were independent of Tg,PS. These results suggest that the mobility of PCL-b-PS influences extremely the crystallizability of the PCL block, but not the resulting morphology. The morphologies formed in the plasticizer-added PCL-b-PS were compared with those of PCL-b-PS cast from toluene or cyclohexane solution, and the characteristics of these morphologies were qualitatively discussed." @default.
• W2064596567 created "2016-06-24" @default.
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• W2064596567 date "1998-01-01" @default.
• W2064596567 modified "2023-10-18" @default.
• W2064596567 title "The effect of glass transition temperature on the crystallization of ε-caprolactone-styrene diblock copolymers" @default.
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• W2064596567 doi "https://doi.org/10.1016/s0032-3861(97)00457-6" @default.
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