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- W2064716888 abstract "The tetraphenylstibonium sulphonates Ph4SbO3SR·nH2O (n = 1, R = C6H5; n = 0, R = CH3, CF3, CH2CH2OH, 4-CH3C6H4, 2,4(NO2)2C6H3) have been obtained by neutralization of tetraphenylstibonium hydroxide with the appropriate alkyl- or aryl-sulphonic acid. The crystal structure of tetraphenylstibonium benzenesulfonate hydrate has been determined by single crystal X-ray diffraction. The sulphonate group is unidentately coordinated to antimony, which has a distorted trigonal bipyramidal environment. The rather long SbO bond, (2.506(4) Å) and the distortion of the polyhedron around Sb, and the IR data for the sulphonate group are consistent with the assumption of a large ionic bond character in the SbO bond. From IR data analogous molecular structures are inferred for the other tetraphenylstibonium sulphonates." @default.
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- W2064716888 date "1985-11-01" @default.
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- W2064716888 title "Synthesis of tetraphenylstibonium alkyl- and aryl- sulphonates. Crystal structure of tetraphenylstibonium benzenesulphonate hydrate" @default.
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- W2064716888 doi "https://doi.org/10.1016/0022-328x(85)88068-2" @default.
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