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- W2064761189 abstract "Abstract A method has been established for the structural analysis of polysaccharides, involving the application in sequence of periodate oxidation, hypoiodite oxidation, and acid hydrolysis. The resulting products have been separated by anion-exchange chromatography. L -Lactic acid was determined by reaction with lactic acid dehydroganese and total lactic acid by conversion into acetaldehyde. Oxidation of the “polyaldehyde” to the “polyacid” with hypoiodite gave higher yields than use of bromine in the presence of strontium carbonate. Methyl α- L -rhamnopyranoside, on degradation, gave L -lactic acid and glyoxylic acid, whereas methyl 6-deoxy-α- D -allopyranoside yielded D -lactic acid and glyoxylic acid. Methyl α- D -glucopyranoside, on degradation, gave glyceric acid, the reactions of which were consistent with its being the D -isomer. Degradation of the polysaccharide nigeran gave equimolar amounts of erythronic acid and glucose." @default.
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- W2064761189 date "1972-05-01" @default.
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- W2064761189 title "Structural analysis by hypoiodite oxidation of periodate-oxidised carbohydrates" @default.
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- W2064761189 doi "https://doi.org/10.1016/s0008-6215(00)81278-1" @default.
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