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- W2064793075 abstract "Reverse-phase high-performance liquid chromatographic (RP-HPLC) separation and analysis of polydisperse water-soluble gold nanoclusters (AuNCs) stabilised with N,N'-dimethylformamide (DMF) were investigated. Under optimal elution gradient conditions, the separation of DMF-AuNCs was monitored by absorption and fluorescence spectroscopy. The UV-vis spectral characteristics of the separated DMF-AuNCs have been captured and they do not possess distinct surface plasmon resonance bands, indicating that all DMF-AuNCs are small AuNCs. The photoluminescence emission spectra of the separated DMF-AuNCs are in the blue-light region. Moreover, cationic DMF-AuNCs are for the first time identified by ion chromatography. Our proposed RP-HPLC methodology has been successfully applied to separate AuNCs of various Au atoms as well as DMF-stabilised ligands. Finally, the composition of the separated DMF-AuNCs was confirmed by matrix-assisted laser desorption/ionisation time-of-flight mass spectrometry and electrospray ionisation mass spectrometry, proving that the as-synthesised DMF-AuNCs product consists of Au₁₀⁺, Au₁₀, Au₁₁, Au₁₂, Au₁₃, and Au₁₄ NCs stabilised with various numbers of DMF ligands." @default.
- W2064793075 created "2016-06-24" @default.
- W2064793075 creator A5006272236 @default.
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- W2064793075 date "2012-01-01" @default.
- W2064793075 modified "2023-10-08" @default.
- W2064793075 title "High-performance liquid chromatographic analysis of as-synthesised N,N′-dimethylformamide-stabilised gold nanoclusters product" @default.
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- W2064793075 doi "https://doi.org/10.1039/c2nr30984j" @default.
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