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• W2064915101 abstract "A simple route to synthesize a new type of phosphorus-containing polyhedral oligomeric silsesquioxanes (DOPO–POSS) in high yield, by the hydrolytic condensation of a modified silane, is reported. The starting material was a phosphorus-containing triethoxy silane (DOPO–VTES), which was synthesized by addition reaction between 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) and vinyl triethoxy silane (VTES). This product was subjected to hydrolytic condensation using an HCl catalyst in methanol. The new types of phosphorus-containing POSS were obtained and characterized using 1H, 13C, 29Si-NMR, MALDI-TOF MS, XRD, DSC, and FTIR. All of these results suggested that the DOPO–POSS were amorphous mixtures of T8, T9(OH), and TGA curve of DOPO–POSS shows that the cage-like compound has high thermal stability. © 2011 Wiley Periodicals, Inc. J Appl Polym Sci, 2011" @default.
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• W2064915101 date "2011-07-12" @default.
• W2064915101 modified "2023-09-28" @default.
• W2064915101 title "Synthesis of phosphorus-containing polyhedral oligomeric silsesquioxanes via hydrolytic condensation of a modified silane" @default.
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• W2064915101 doi "https://doi.org/10.1002/app.34471" @default.
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