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- W2064935750 abstract "Nano-sized TiO2 powders were prepared by controlled hydrolysis of TiCl4 and Ti(O-i-C3H7)4 solutions and nitrided in flowing NH3 gas at 700°–1000°C to form TiN. Nano-sized TiN was densified by spark plasma sintering at 1300°–1600°C to produce TiN ceramics with a relative density of 98% at 1600°C. The microstructure of the etched ceramic surface was observed by SEM, which revealed the formation of uniformly sized 1–2 μm grains in the TiCl4-derived product and 10–20 μm in the Ti(O-i-C3H7)4-derived TiN. The electric resisitivity and Vickers micro-hardness of the TiN ceramics was also measured." @default.
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- W2064935750 date "2003-09-01" @default.
- W2064935750 modified "2023-10-18" @default.
- W2064935750 title "Spark Plasma Sintering of Nano-Sized TiN Prepared from TiO<sub>2</sub>by Controlled Hydrolysis of TiCl<sub>4</sub>and Ti(O-i-C<sub>3</sub>H<sub>7</sub>)<sub>4</sub>Solution" @default.
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- W2064935750 doi "https://doi.org/10.1111/j.1151-2916.2003.tb03524.x" @default.
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