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- W2064961808 abstract "Abstract The formation mechanism and microstructural development of the spinel phases in the Co 1 − x O/Co 2 TiO 4 composites upon reactive sintering the Co 1 − x O and TiO 2 powders (9:1 molar ratio) at 1450 °C and during subsequent cooling in air were studied by X-ray diffraction and analytical electron microscopy. The Co 2 TiO 4 spinel occurred as inter- and intragranular particles in the matrix of Ti-doped Co 1 − x O grains with a rock salt-type structure during reactive sintering. The submicron sized Co 2 TiO 4 particles were able to detach from grain boundaries in order to reach an energetically favorable parallel orientation with respect to the host Co 1 − x O grains via a Brownian-type rotation/coalescence process. Upon cooling in air, secondary Co 2 TiO 4 nanoparticles were precipitated and the Ti-doped Co 1 − x O host was partially oxidized as Co 3 − δ O 4 spinel by rapid diffusion along the {1 1 1} and {1 0 0}-decorated interphase interface and the free surface of the composites." @default.
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- W2064961808 date "2011-05-01" @default.
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- W2064961808 title "On the spinel formation in Co1−xO/Co2TiO4 composites via reactive sintering, exsolution and oxidation" @default.
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- W2064961808 doi "https://doi.org/10.1016/j.ceramint.2010.12.011" @default.
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