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- W2065005105 abstract "A cation-exchange column packed with CM-Sephadex C25 matrix was evaluated for its efficiency, capacity, elution volume, and reproducibility in purifying crude extracts of rapeseed or meal for the determination of sinapine content. Combined with a single extraction and ion-exchange column purification procedure, sinapine content in the seed or meal could be quantified with a coefficient of variance of 3.9%. Recovery of sinapine from rapeseed or meal using this method was 95-114% with a lower limit of the sinapine detection of 2.5 µg/mL. The proposed method is not labor-intensive and is applicable to batch analysis of up to 120 samples per day, thereby reducing the cost of analysis." @default.
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- W2065005105 title "Application and Evaluation of Ion-Exchange UV Spectrophotometric Method for Determination of Sinapine in <i>Brassica</i> Seeds and Meals" @default.
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- W2065005105 doi "https://doi.org/10.1021/jf9705577" @default.
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