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- W2065011402 abstract "A reliable method for the microdetermination of cobalt in organic cobalt compounds is described. The sample is combusted in a modified oxygen flask and the products are absorbed in 6 M HC1. The Pt basket is then boiled in the absorption solution and the sparingly soluble residue of cobalt oxides is completely dissolved. After cooling, the solution is transferred to a titration cell and neutralized with NaOH in the presence of methyl red. After careful adjustment of the pH, the Co(II) is finally determined in a buffered 60% (vv) dimethylformamide solution by potentiometric titration with 0.033 M sodium diethyldithiocarbamate solution. The results obtained are accurate within ±0.08%; the recoveries of Co are in the range of 99.52 to 99.97%; the standard deviation is 0.06%. The potentiometric titration of Co(II) with sodium diethyldithiocarbamate and other reagents, as well as the conditions for the oxygen flask combustion of organic cobalt compounds, is discussed." @default.
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- W2065011402 date "1992-10-01" @default.
- W2065011402 modified "2023-10-18" @default.
- W2065011402 title "The potentiometric microdetermination of cobalt in organic compounds after combustion in a modified oxygen flask" @default.
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- W2065011402 doi "https://doi.org/10.1016/0026-265x(92)90041-z" @default.
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