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- W2065049868 abstract "Films consisting of a vanadium pentoxide (i.e., V2O5) phase formed within a rubbery block copolymer were developed for their potential use as nanocomposite cathodes in lithium rechargeable batteries. Nanocomposite films were prepared by sol−gel synthesis from vanadyl triisopropoxide precursor in poly(oligooxyethylene methacrylate)-block-poly(butyl methacrylate), POEM-b-PBMA. The in situ growth of amorphous V2O5 was confirmed by wide-angle X-ray scattering (WAXS), X-ray photoelectron spectroscopy (XPS), and small-angle X-ray scattering (SAXS). Scanning transmission electron microscopy (STEM) and differential scanning calorimetry (DSC) demonstrated the selective incorporation of vanadium oxide within the ion-conducting POEM domains, while the oxide morphology was revealed by TEM to be a filamentous network. Cyclic voltammetry and impedance spectroscopy confirmed the preservation of the redox properties of the vanadium oxide and the ion-conductive properties of the polymer in hybrid films. Co-assembled nanocomposite films incorporating up to 34 wt % (13 vol %) vanadium oxide were flexible and semi-transparent." @default.
- W2065049868 created "2016-06-24" @default.
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- W2065049868 date "2006-05-16" @default.
- W2065049868 modified "2023-10-18" @default.
- W2065049868 title "Sol−Gel Synthesis of Vanadium Oxide within a Block Copolymer Matrix" @default.
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- W2065049868 doi "https://doi.org/10.1021/cm060119s" @default.
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