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• W2065166672 abstract "Site-differentiated solvated clusters of the general formula [Re(6)(mu(3)-Se)(8)(PEt(3))(n)(MeCN)(6)(-)(n)](SbF(6))(2) (n = 4, cis and trans; n = 5) undergo ligand substitution reaction with isonicotinamide to afford the corresponding amide derivatives, [Re(6)(mu(3)-Se)(8)(PEt(3))(n)(isonicotinamide)(6)(-)(n)](2+) [1 (n = 5); 2 (n = 4, trans); 3 (n = 4, cis)]. Retention of stereochemistry in each case was confirmed by (1)H and (31)P NMR. The solid-state structures of all three compounds were established crystallographically, which revealed self-complementary hydrogen-bonding interactions between adjacent cluster units. While complex 1 exists as hydrogen-bonded dimers in the solid state, compounds 2 and 3 form one-dimensional chains of clusters bridged by paired hydrogen bonds. It is the rigid stereochemistry of the cluster, combined with the classic crystal engineering motif of complementary N-H.O amide hydrogen bonding, that affords the predictable solid-state structures and dimensionality." @default.
• W2065166672 created "2016-06-24" @default.
• W2065166672 creator A5000047639 @default.
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• W2065166672 date "2003-02-08" @default.
• W2065166672 modified "2023-10-03" @default.
• W2065166672 title "Hydrogen-Bonded Extended Arrays of the [Re₆(μ₃-Se)₈]²⁺ Core-Containing Clusters" @default.
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• W2065166672 doi "https://doi.org/10.1021/ic0261326" @default.
• W2065166672 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/12611536" @default.
• W2065166672 hasPublicationYear "2003" @default.
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