FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W2065283988> ?p ?o ?g. }

• W2065283988 endingPage "31" @default.
• W2065283988 startingPage "23" @default.
• W2065283988 abstract "A selective and sensitive liquid chromatography tandem mass spectrometric (LC–MS/MS) method has been developed for simultaneous determination of residual bacitracin and colistin in bovine milk samples. Milk samples were deproteinized and extracted with a mixture of trichloroacetic/formic acid. After centrifugation, bacitracin and colistin in the extracts were separated on a reversed phase Alltima BDS C18 column (250 mm × 2.1 mm, 5 μm) using a gradient elution programme of ammonium formate buffer (saturated ammonium formate:formic acid:acetonitrile:water, 1:5:50:950, v/v/v/v) and 0.1% formic acid in acetonitrile at 0.2 ml min−1. Using electrospray LC–MS/MS with time-scheduled multiple reaction monitoring (MRM), identification and quantification of the major components of the two polypeptides were performed based upon the intensities of mass fragments from the respective doubly charged precursor ions: bacitracin A at 712 → 199 amu and 712 → 227 amu, and colistin A at 586 → 101 amu, 586 → 202 amu and 586 → 241 amu, respectively, at the defined retention time windows and the matching of the specific tolerance of the relative abundance of the monitored ions. Polymyxin B, a polypeptide of colistin family, was employed as the internal standard. With an additional solid phase extraction procedure, the analytical method was applicable to the analysis of the two polypeptide antibiotics in animal's liver and tissue samples. The practical quantification limits of bacitracin A and colistin A were 100 and 50 μg kg−1; and mean intra-day (n = 7) and inter-day (n = 4) recoveries were in the range of 89.2–110% (R.S.D. < 10%), and 90.4–112% (R.S.D. < 13%) respectively in all matrices." @default.
• W2065283988 created "2016-06-24" @default.
• W2065283988 creator A5007662826 @default.
• W2065283988 creator A5020585476 @default.
• W2065283988 creator A5021093924 @default.
• W2065283988 creator A5055798768 @default.
• W2065283988 creator A5057329175 @default.
• W2065283988 date "2005-04-01" @default.
• W2065283988 modified "2023-09-27" @default.
• W2065283988 title "Analysis of major components of residual bacitracin and colistin in food samples by liquid chromatography tandem mass spectrometry" @default.
• W2065283988 cites W1973405486 @default.
• W2065283988 cites W1973518816 @default.
• W2065283988 cites W1992631904 @default.
• W2065283988 cites W1994434948 @default.
• W2065283988 cites W2007996059 @default.
• W2065283988 cites W2009237075 @default.
• W2065283988 cites W2018074392 @default.
• W2065283988 cites W2019892872 @default.
• W2065283988 cites W2020717334 @default.
• W2065283988 cites W2026391790 @default.
• W2065283988 cites W2039864229 @default.
• W2065283988 cites W2043308376 @default.
• W2065283988 cites W2048356379 @default.
• W2065283988 cites W2051114685 @default.
• W2065283988 cites W2055755751 @default.
• W2065283988 cites W2075101032 @default.
• W2065283988 cites W2090456048 @default.
• W2065283988 cites W2144783676 @default.
• W2065283988 cites W2154467619 @default.
• W2065283988 cites W2156510510 @default.
• W2065283988 cites W2162745520 @default.
• W2065283988 doi "https://doi.org/10.1016/j.aca.2004.11.063" @default.
• W2065283988 hasPublicationYear "2005" @default.
• W2065283988 type Work @default.
• W2065283988 sameAs 2065283988 @default.
• W2065283988 citedByCount "52" @default.
• W2065283988 countsByYear W20652839882012 @default.
• W2065283988 countsByYear W20652839882013 @default.
• W2065283988 countsByYear W20652839882014 @default.
• W2065283988 countsByYear W20652839882015 @default.
• W2065283988 countsByYear W20652839882016 @default.
• W2065283988 countsByYear W20652839882017 @default.
• W2065283988 countsByYear W20652839882018 @default.
• W2065283988 countsByYear W20652839882019 @default.
• W2065283988 countsByYear W20652839882020 @default.
• W2065283988 countsByYear W20652839882021 @default.
• W2065283988 countsByYear W20652839882022 @default.
• W2065283988 crossrefType "journal-article" @default.
• W2065283988 hasAuthorship W2065283988A5007662826 @default.
• W2065283988 hasAuthorship W2065283988A5020585476 @default.
• W2065283988 hasAuthorship W2065283988A5021093924 @default.
• W2065283988 hasAuthorship W2065283988A5055798768 @default.
• W2065283988 hasAuthorship W2065283988A5057329175 @default.
• W2065283988 hasConcept C161790260 @default.
• W2065283988 hasConcept C162356407 @default.
• W2065283988 hasConcept C185592680 @default.
• W2065283988 hasConcept C2775986502 @default.
• W2065283988 hasConcept C2777379063 @default.
• W2065283988 hasConcept C2779259085 @default.
• W2065283988 hasConcept C2779860364 @default.
• W2065283988 hasConcept C2780178953 @default.
• W2065283988 hasConcept C31827203 @default.
• W2065283988 hasConcept C43617362 @default.
• W2065283988 hasConcept C4725764 @default.
• W2065283988 hasConcept C501593827 @default.
• W2065283988 hasConcept C55493867 @default.
• W2065283988 hasConcept C64489805 @default.
• W2065283988 hasConcept C71043704 @default.
• W2065283988 hasConcept C81426234 @default.
• W2065283988 hasConceptScore W2065283988C161790260 @default.
• W2065283988 hasConceptScore W2065283988C162356407 @default.
• W2065283988 hasConceptScore W2065283988C185592680 @default.
• W2065283988 hasConceptScore W2065283988C2775986502 @default.
• W2065283988 hasConceptScore W2065283988C2777379063 @default.
• W2065283988 hasConceptScore W2065283988C2779259085 @default.
• W2065283988 hasConceptScore W2065283988C2779860364 @default.
• W2065283988 hasConceptScore W2065283988C2780178953 @default.
• W2065283988 hasConceptScore W2065283988C31827203 @default.
• W2065283988 hasConceptScore W2065283988C43617362 @default.
• W2065283988 hasConceptScore W2065283988C4725764 @default.
• W2065283988 hasConceptScore W2065283988C501593827 @default.
• W2065283988 hasConceptScore W2065283988C55493867 @default.
• W2065283988 hasConceptScore W2065283988C64489805 @default.
• W2065283988 hasConceptScore W2065283988C71043704 @default.
• W2065283988 hasConceptScore W2065283988C81426234 @default.
• W2065283988 hasIssue "1-2" @default.
• W2065283988 hasLocation W20652839881 @default.
• W2065283988 hasOpenAccess W2065283988 @default.
• W2065283988 hasPrimaryLocation W20652839881 @default.
• W2065283988 hasRelatedWork W1990710770 @default.
• W2065283988 hasRelatedWork W1992561179 @default.
• W2065283988 hasRelatedWork W2001353325 @default.
• W2065283988 hasRelatedWork W2092328469 @default.
• W2065283988 hasRelatedWork W2351302509 @default.
• W2065283988 hasRelatedWork W2386455741 @default.
• W2065283988 hasRelatedWork W2635418940 @default.
• W2065283988 hasRelatedWork W2739744284 @default.
• W2065283988 hasRelatedWork W2911397462 @default.

• next