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• W2065354712 abstract "The present study has concentrated on finding a new stationary phase in liquid chromatography. To improve the selectivity of monolithic column, a new ionic liquids–based (ILs-based) monolithic column (150 × 4.6 mm i.d.) is synthesized. Characteristic and evaluation of monolithic column are investigated by field emission-scanning electron microscopy (FE-SEM) and determination of caffeine and theophylline in high performance liquid chromatography (HPLC). FE-SEM images show that this monolithic column has a porosity structure. At the condition of mobile phase was 0.06 mol L−1 Na2HPO4 (pH 9.0) and flow rate was 0.7 mL min−1, a good linear relationship was demonstrated when the concentrations of caffeine and theophylline were in the range of 0.1–60.0 μg mL−1. These two compounds can obtain better resolution on the ILs-based monolithic column than non-ILs monolithic column, and the recoveries ranged from 97.40% to 108.00% and the interday and intraday relative standard deviations were less than 5%. The HPLC method, developed in this study, was proved to be acceptable for drugs assay, and this ILs-based monolithic column as the stationary phase was a potential tool for future HPLC separation. © 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2010" @default.
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• W2065354712 date "2010-07-14" @default.
• W2065354712 modified "2023-09-27" @default.
• W2065354712 title "A new ionic liquids-based monolithic column for determination of caffeine and theophylline" @default.
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• W2065354712 doi "https://doi.org/10.1002/app.32684" @default.
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