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- W2065432454 abstract "The dimeric copper(I) 3-sila-β-diketiminate [Cu{(N(R)C(Ar)) 2 SiR}] 2 · (thf) ( 1 ) was obtained from CuI and [Li{(N(R)C(Ar)) 2 SiR}(thf) 2 ] ( B ) in toluene (R = SiMe 3 , Ar = C 6 H 3 Me 2 -2,6). When [CuI(PPh 3 ) 3 ] was used as a starting material, the LiI-containing compound [Cu{Si(R)(C(Ar)N(R)) 2 Li(μ-I)}(PPh 3 )] ( 2 ) was isolated. The reaction of [MI(PPh 3 ) n ] (M = Ag, n = 3; M = Au, n = 2) with two equivalents of B in toluene gave the isomorphous silver and gold 3-sila-β-diketiminates [M{Si(R)(C(Ar)N(R)) 2 Li} 2 (μ-I)] [M = Ag ( 3 ), Au ( 4 )]. Each of 1 – 4 was characterised by the multinuclear NMR spectroscopy and single-crystal X-ray diffraction crystallography." @default.
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- W2065432454 date "2007-10-01" @default.
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- W2065432454 title "Synthesis and structures of 3-sila-β-diketiminato complexes of the coinage metals" @default.
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- W2065432454 doi "https://doi.org/10.1016/j.jorganchem.2007.07.012" @default.
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