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- W2065514296 abstract "Samples of poly(trimethylhexamethylene terephthalamide) were first blended with separately prepared fumed silica in the absence of a coupling agent, and their mechanical properties were measured in continuous extension. The reinforcement obtained in this ex situ approach was qualitatively similar to that obtained by the in situ generation of silica in the sol–gel hydrolysis and condensation of tetraethoxysilane. The increase of ultimate (tensile) strength, however, was only 10%, compared to the 25% obtained in the in situ approach. Adding 20 or 40 mol% of an epoxysilane coupling agent to the ex situ samples gave increases in tensile strength up to 50%. Scanning electron microscopy showed interesting differences in the structures of these various fillers. For example, the fumed silica particles without the coupling agent showed a tendency to form heterogeneous aggregates in a spherical texture. The particles coated with the coupling agent showed little aggregation and evidence of good adhesion to the polya..." @default.
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- W2065514296 date "2000-11-25" @default.
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- W2065514296 title "REINFORCEMENT OF THE AROMATIC POLYAMIDE POLY(TRIMETHYLHEXAMETHYLENE TEREPHTHALAMIDE): COMPARISONS AMONG BLENDED EX SITU SILICA WITH AND WITHOUT A BONDING AGENT AND IN SITU GENERATED SILICA" @default.
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- W2065514296 doi "https://doi.org/10.1081/ppt-100101410" @default.
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