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• W2065526137 abstract "In the present research, a modified post-hydrothermal treatment with different temperature of 80-150°C has been applied on as-annealed TiO 2 nanotubes derived from conventional hydrothermal process. The treatment has two-fold objectives, i.e. enhancing the nanocrystallinity of anatase TiO 2 , and at the same time maintaining the integrity of nanotube structures. The resulting TiO 2 nanotubes were characterized by using XRD and UV-Vis spectroscopy. The XRD analysis revealed that the as dried TiO 2 nanotubes contain combined crystalline structures of sodium-titanate and anatase. It was also found that by increasing the post-hydrothermal temperature from 80 to 150°C, the nanocrystallinity of nanotubes enhances as indicated by increasing the crystallite size of anatase TiO 2 from 6.93 to 7.81 nm. The anatase crystallite growth affected the optical characteristic of nanotubes, as represented with the reduction of the band gap energy, E g from 3.75 to 3.67 eV by using Kubelka-Munk analysis for the obtained UV-Vis reflectance spectra. TEM observation confirms that the integrity of nanotubes structure can be well-maintained upon post-hydrothermal treatment." @default.
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• W2065526137 date "2011-07-01" @default.
• W2065526137 modified "2023-10-04" @default.
• W2065526137 title "Nanocrystallinity Enhancement of TiO₂ Nanotubes by Post-Hydrothermal Treatment" @default.
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• W2065526137 doi "https://doi.org/10.4028/www.scientific.net/amr.277.90" @default.
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