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- W2065619234 abstract "Partially amorphous powders of the alloy Fe75Si15B10 were formed by gas-water atomization. Both an ultrasonic nozzle and an annular nozzle were used and the yields of various size fractions were compared. The crystallization characteristics were investigated by differential scanning calorimetry and compared with the crystallization characteristics of chill-cast ribbon and spark-eroded powder of the same composition. The magnetic properties were also compared. X-ray diffraction and magnetization at 4.2 K revealed that the gas-water-atomized particles were mostly amorphous in the size range less than 10 μm but were about 50% crystalline in the size range 20–30 μm. The crystals were α-Fe and Fe3Si. The atomized particles contained cellular crystals that nucleated and grew on solidification as well as crystals that nucleated and grew in the amorphous phase. It was concluded that the cooling rate for gas-water atomization is lower than that for the chill-cast ribbon (106 K s−1) which accounts for the presence of crystals in the atomized particles. The properties of the amorphous phase of the atomized particles are the same as for the ribbon but are different from the properties of the amorphous spark-eroded particles. The chemical short-range order of the amorphous phase of the atomized particles is like that of the ribbon but different from that of the more rapidly cooled spark-eroded particles." @default.
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- W2065619234 date "1984-02-01" @default.
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- W2065619234 title "Structures and properties of powders of Fe75Si15B10 produced by gas-water atomization" @default.
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- W2065619234 doi "https://doi.org/10.1016/0025-5416(84)90225-8" @default.
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