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• W2065760464 abstract "As a step towards the structural analysis of the carotenoid spheroidene in the Rhodobacter sphaeroides reaction centre, we present the resonance Raman spectra of 14-2H, 15-2H, 15′-2H, 14′-2H, 14,15′-2H2, and 15,15′-2H2 spheroidenes in petroleum ether and, except for 14,15′-2H2 spheroidene, in the Rb. sphaeroides R26 reaction center (RC). Analysis of the spectral changes upon isotopic substitution allows a qualitative assignment of most of the vibrational bands to be made. For the all-trans spheroidenes in solution the resonance enhancement of the Raman bands is determined by the participation of carbon-carbon stretching modes in the centre of the conjugated chain, the C9 to C15′ region. For the RC-bound 15,15′-cis spheroidenes, enhancement is determined by the participation of carbon-carbon stretching modes in the centre of the molecule, the C13 to C13′ region. Comparison of the spectra in solution and in the RC reveals evidence for an out-of-plane distortion of the RC-bound spheroidene in the central C14 to C14′ region of the carotenoid. The characteristic 1240 cm−1 band in the spectrum of the RC-bound spheroidene has been assigned to a normal mode that contains the coupled C12C13 and C13′C12′ stretch vibrations." @default.
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• W2065760464 date "1997-03-01" @default.
• W2065760464 modified "2023-09-30" @default.
• W2065760464 title "Resonance Raman spectroscopy of 2H-labelled spheroidenes in petroleum ether and in the Rhodobacter sphaeroides reaction centre" @default.
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• W2065760464 doi "https://doi.org/10.1016/s1386-1425(96)01845-8" @default.
• W2065760464 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/9177038" @default.
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