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- W2065888964 abstract "Chrysazin, C14H8O4, crystallized from the solution of the substance in benzene, is tetragonal, space group P41 or P43, with four molecules in a unit cell of dimensions a = 5.76 Å and c = 31.45 Å. The trial structure, which was derived from the considerations of strong reflections, molecular packing and hypersymmetry, has been refined by two-dimensional (100)-Fourier projections followed by a few cycles of difference synthesis and least-squares refinement. The refinement of all the three parameters x, y, z has been done using the 0kl reflections; however, the hk0 reflections were also included in the least-squares refinement. The molecule is planar within the limits of experimental error and the various bond lengths and bond angles agree with those found in similar compounds. All the intermolecular approaches correspond to the normal van der Waals interactions, the closest being 2.68 Å between O1(x,y,z) and O2(x–1, y+1,z). The crystal and molecular structure has been discussed." @default.
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- W2065888964 date "1965-11-01" @default.
- W2065888964 modified "2023-10-12" @default.
- W2065888964 title "The crystal and molecular structure of chrysazin" @default.
- W2065888964 doi "https://doi.org/10.1524/zkri.1965.122.3-4.272" @default.
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