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• W2065932067 endingPage "2362" @default.
• W2065932067 startingPage "2355" @default.
• W2065932067 abstract "Reactions of silver(I) perchlorate with tetraphenyl-cyclopentadiene (Ph4H2C5) have isolated two novel silver(I) bridged tetraphenyl-pyrylium complexes: [Ag(ClO4)(Ph4HC5O+)](ClO4)− (1) and [Ag(ClO4)(H2O)(Ph4HC5O+)](ClO4-) (2), depending on moisture-content of the reactants. Structure studies using single-crystal X-ray diffraction have showed that complex 1 contains a distorted tetrahedral metal center bridging two neighboring peripheral phenyl rings of one pyrylium cation and two perchlorate anions, whereas 2 involves a three-coordinate metal ion interacting with a pair of phenyl rings and one water molecule, leaving two perchlorate anions free from coordination. For both complexes, the precursor ligand Ph4H2C5 undergoes a ring-enlargement reaction, forming a six-membered pyrylium cation. The fundamentals of the synthesis, structure characterization and some properties are discussed." @default.
• W2065932067 created "2016-06-24" @default.
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• W2065932067 date "2005-04-01" @default.
• W2065932067 modified "2023-09-23" @default.
• W2065932067 title "Synthesis and crystal structures of silver(I) bridged tetra-phenyl-pyrylium complexes from tetraphenyl-cyclopentadiene" @default.
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• W2065932067 doi "https://doi.org/10.1016/j.ica.2005.01.009" @default.
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