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• W2066013074 abstract "The mass spectra of arylpentamethyldisiloxanes, sym-diaryltetramethyldisiloxanes and 1,5-diaryl-1,1,3,3,5,5-hexamethyltrisiloxanes were examined. Isotopic labeling and peak matching were used to substantiate the proposed fragmentation mechanisms. Siliconium ions dominate the spectra. Loss of neutral fragments from the [M-15]+ ions is important. Phenylpentamethyldisiloxane, sym-tetramethyldiphenyldisiloxane and 1,1,3,3,5,5-hexamethyl-1,5-diphenyltrisiloxane are representative examples of the three classes of compounds discussed. The [M-15]+ ion of phenylpentamethyldisiloxane loses methane, dimethylsilanone [(CH3)2SiO] and phenylmethylsilanone [PhCH3SiO] to yield daughter siliconium ions. The [M-15]+ ion of sym-tetramethyldiphenyldisiloxane loses benzene, methane, dimethylsilanone and phenylmethylsilanone to yield daughter siliconium ions. The [M-15]+ ion of 1,1,3,3,5,5-hexamethyl-1,5-diphenyltrisiloxane loses benzene, tetramethylcyclodisiloxane and phenyltrimethylcyclodisiloxane to yield daughter siliconium ions. Finally, doubly charged ions are important in the mass spectra of the three series of aryl substituted di- and trisiloxanes discussed." @default.
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• W2066013074 date "1980-06-01" @default.
• W2066013074 modified "2023-10-01" @default.
• W2066013074 title "Mass spectrometry of aryl substituted di- and trisiloxanes" @default.
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• W2066013074 doi "https://doi.org/10.1002/oms.1210150608" @default.
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