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- W2066088081 abstract "Abstract The acetylation reaction of polytetramethylene glycol (PTMG) with acetic anhydride in pyridine was studied. The extent of acetylation was measured by 1 H‐NMR, and the acetylation product was characterized with FTIR, 1 H‐NMR, and 13 C‐NMR. The effects of the experimental conditions, i.e., reaction time and temperature, acetylation reagent concentration (anhydride and hydroxyl molar ratio), were investigated. The increase in reaction temperature and reaction time favored the acetylation yields. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 1138–1142, 2007" @default.
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- W2066088081 date "2007-01-26" @default.
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- W2066088081 title "Acetylation reaction of polytetramethylene glycol with acetic anhydride in pyridine" @default.
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- W2066088081 doi "https://doi.org/10.1002/app.25743" @default.
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