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- W2066162016 abstract "The crystal structure of the title compound has been determined from X-ray diffractometer intensity data and refined by least-squares methods to R 0·068 for 2913 reflexions. The crystals (γ-modification, m.p. 130·5°) are triclinic with a= 10·88 ± 0·03, b= 11·37 ± 0·03, c= 6·30 ± 0·02 A; α= 95·7°, β= 100·2°, γ= 85·4°(all ±0·2°); Z= 1, space group P. The molecule occupies a crystallographic centre of symmetry and the phosphazene ring has the chair conformation, with approximate symmetry 2/m(C2h). Mean bond lengths (A) are : P–N(cyclic) 1·593, P–N(exocyclic) 1·672, and P–C 1·808. There are two different P–N–P angles in the ring: 124·6 and 131·3°. The molecule is very similar in shape to that of its parent compound N4P4Cl4Ph4." @default.
- W2066162016 created "2016-06-24" @default.
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- W2066162016 date "1972-01-01" @default.
- W2066162016 modified "2023-09-24" @default.
- W2066162016 title "Molecular structures of non-geminally substituted phosphazenes. Part I. Crystal structure of 2,cis-4,trans-6,trans-8-tetrakismethylamino-2,4,6,8-tetraphenylcyclotetraphosphazene" @default.
- W2066162016 doi "https://doi.org/10.1039/dt9720001412" @default.
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