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• W2066339768 abstract "Reaction of various N-substituted diethanolamines H2L3 (4) with calcium hydride and iron(III) chloride leads to the self-assembly of six-membered ferric wheels [Fe6X6(L3)6] (5). Principally, all the iron coronands are isostructural; however, they differ fundamentally with respect to their crystal packing. Exemplarily, this is discussed for selected members of the space groups R3̄, P3̄, P21/c, P21/n, C2/c, and P1̄. Depending on the nature of their sidearms, the ferric wheels create various substructures. For instance, the ferric wheels 5a−i of space group R3̄ or P3̄ are piled in parallel in cylindrical columns, which are surrounded by six parallel columns alternately dislocated by 1/3c and 2/3c against the central one. Pronounced van der Waals interactions give rise to compartmentation and incarceration of guest molecules as seen for 5e,g. However, in 5h strong π−π interactions create a three-dimensional scaffold. The most significant difference of the ferric wheels 5j−p of space groups P21/c, P21/n, and C2/c is that these ferric wheels are arranged in parallel in two orientations. They differ mainly only by the included angle of the two groups of parallel wheels. In the case of 5l, molecular chains are formed in the crystal due to π−π interactions. The ferric wheels 5q−y of space group P1̄ are packed in the crystal most simply, with all the ferric wheels piled in parallel." @default.
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• W2066339768 date "2004-06-05" @default.
• W2066339768 modified "2023-10-17" @default.
• W2066339768 title "Six-Membered Metalla-coronands. Synthesis and Crystal Packing: Columns, Compartments, and 3D-Networks^," @default.
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• W2066339768 doi "https://doi.org/10.1021/ic049799w" @default.
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