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- W2066802210 abstract "Abstract The ion-exchange behaviour of the lamellar phosphatoantimonate phases, A 3 Sb 3 P 2 O 14 · Z H 2 O (A = H, K; Z = 5, 6) in acidic media has been explored for several trivalent lanthanides (La 3+ , Eu 3+ and Pr 3+ ) and the actinide 241 Am 3+ . The protonated phase displayed high levels of uptake for each of these cations in mildly acidic media ( 3 ) and was also shown to be tolerant of moderate levels of potassium cations. The La 3+ ↔ 3H 3 O + exchange has been further studied using thermogravimetric, variable temperature X-ray diffraction, FT-IR and 31 P MAS NMR. Difficulties in drawing conclusions regarding the siting of La 3+ at one or both of the unique ion-exchange sites of the {Sb 3 P 2 O 14 } ∞ framework were experienced due to complications arising from the presence of intercalated water. This study has demonstrated that the exchange of La 3+ leads to a proportion of the ion-exchange sites about some of the PO 4 tetrahedra being left vacant upon exchange. The utility of the phosphatoantimonate framework for removal of radiogenic lanthanide and americium from acidic media has been demonstrated." @default.
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- W2066802210 date "2008-04-01" @default.
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- W2066802210 title "Lanthanide/actinide ion-exchange and structural investigations of the layered phosphatoantimonic acid, H3Sb3P2O14·ZH2O" @default.
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- W2066802210 doi "https://doi.org/10.1016/j.micromeso.2007.08.028" @default.
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