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• W2067033430 endingPage "1989" @default.
• W2067033430 startingPage "1982" @default.
• W2067033430 abstract "Copper zirconium phosphate nanoparticles have been used as an efficient catalyst for the acetylation of a wide range of alcohols and phenols with acetic anhydride in good to excellent yields under solvent-free conditions. The steric and electronic properties of the different substrates had a significant influence on the reaction conditions required to achieve the acetylation. The catalyst used in the current study was characterized by inductively-coupled plasma optical emission spectroscopy, energy dispersive spectroscopy, X-ray diffraction, N 2 adsorption-desorption, scanning electron microscopy, and transmission electron microscopy. These analyses revealed that the interlayer distance in the catalyst increased from 7.5 to 8.0 Å when Cu 2+ was intercalated between the layers, whereas the crystallinity of the material was reduced. This nanocatalyst could also be recovered and reused at least six times without any discernible decrease in its catalytic activity. This new method for the acetylation of alcohols and phenols has several key advantages, including mild and environmentally friendly reaction conditions, as well as good to excellent yields and a facile work-up. Copper zirconium phosphate was prepared and used as an efficient and reusable nanocatalyst for the acetylation of alcohols with fairyields. The method conforms to several of the guiding principles of green chemistry." @default.
• W2067033430 created "2016-06-24" @default.
• W2067033430 creator A5014623484 @default.
• W2067033430 creator A5079251079 @default.
• W2067033430 date "2014-12-01" @default.
• W2067033430 modified "2023-10-18" @default.
• W2067033430 title "Acetylation of alcohols and phenols under solvent-free conditions using copper zirconium phosphate" @default.
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• W2067033430 doi "https://doi.org/10.1016/s1872-2067(14)60185-6" @default.
• W2067033430 hasPublicationYear "2014" @default.
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