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• W2067042362 abstract "The molecular orientation in self-assembled fims of methyl-, hydroxyl-, and carboxylic acid-terminated alkanethiols of different chain lengths (n-docosanethiol [DCT], 22-mercaptodocosanol [MDO], 22-mercaptodocosanoic acid [MDC], n-hexadecanethiol [HDT], 16-mercaptohexadecanol [MHO], 16-mercaptohexadecanoic acid [MHC]) on Au substrates has been investigated by near edge X-ray absorption fine structure (NEXAFS) spectroscopy and X-ray photoelectron spectroscopy (XPS). Whereas XPS-measurements do not reveal changes in thickness upon replacing the endgroups, the degree of orientation as determined with NEXAFS exhibits significant differences. The two methyl-terminated thiols show the same alkyl-chain tilt-angle α of 39°. For the short-chain OH-terminated films no significant difference could be detected, but the monolayers formed from the long-chain OH-terminated chains exhibit a slightly stronger anisotropy and thus a smaller tilt-angle α than the corresponding CH3-terminated thiol. NEXAFS-spectra recorded for films from COOH-terminated thiols reveal only a very small anisotropy which indicates the absence of significant molecular orientation resulting from a high degree of disorder." @default.
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• W2067042362 date "1997-10-01" @default.
• W2067042362 modified "2023-10-06" @default.
• W2067042362 title "An orientation analysis of differently endgroup-functionalised alkanethiols adsorbed on Au substrates" @default.
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• W2067042362 doi "https://doi.org/10.1016/s0040-6090(97)00280-0" @default.
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