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- W2067203648 abstract "Abstract A convenient and practical synthesis of trimethylamine acrylimide, 1 , starting from 1, 1, 1‐trimethylhydrazinium p ‐toluenesulfonate, 3 , and 3‐chloropropionyl chloride is described. The intermediate, trimethylamine 3‐chloropropionimide, 2 , is easily transformed into 1 either through a single‐step dehydrohalogenation or through a two‐step process consisting of very facile thermal rearrangement to 1,1,1‐trimethylacrylylhydrazinium chloride, 4 , and subsequent deprotonation. Two new polymerizable monomers, 5 , and 6 , containing aminimide functionality were synthesized from trimethylamine imine, 7 , and the appropriate vinyl oxazolones, 8 , and 9 . Synthesis of hitherto unreported trimethylamine chloroacetimide, 10 , which offers unique opportunities for incorporating water‐solubilizing and alkali‐stable aminimide functionality into a variety of structures through nucleophilic displacement, is also described." @default.
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- W2067203648 date "1983-04-01" @default.
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- W2067203648 title "Synthesis of aminimide monomers and polymers" @default.
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- W2067203648 doi "https://doi.org/10.1002/pol.1983.170210422" @default.
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