Matches in SemOpenAlex for { <https://semopenalex.org/work/W2067219679> ?p ?o ?g. }
Showing items 1 to 99 of
99
with 100 items per page.
- W2067219679 endingPage "858" @default.
- W2067219679 startingPage "854" @default.
- W2067219679 abstract "A novel and fast simultaneous determination of triamcinolone acetonide (TCA) and salicylic acid (SA) in topical pharmaceutical formulations by sequential injection chromatography (SIC) as an alternative to classical high performance liquid chromatography (HPLC) has been developed. A recently introduced Onyxtrade mark monolithic C18 (50mmx4.6mm, Phenomenex((R))) with 5mm monolithic precolumn were used for the first time for creating sequential injection chromatography system based on a FIAlab((R)) 3000 with a six-port selection valve and 5.0mL syringe pump in study. The mobile phase used was acetonitrile/water (35:65, v/v), pH 3.3 adjusted with acetic acid at flow rate 0.9mLmin(-1). UV detection provided by fibre-optic DAD detector was set up at 240nm. Propylparaben was chosen as suitable internal standard (IS). There is only simple pre-adjustment of the sample of topical solution (dilution with mobile phase) so the analysis is not uselessly elongated. Parameters of the method showed good linearity in wide range, correlation coefficient >0.999; system precision (relative standard deviation, R.S.D.) in the range 0.45-1.95% at three different concentration levels, detection limits (3sigma) 1.00mugmL(-1) (salicylic acid), 0.66mugmL(-1) (triamcinolone acetonide) and 0.33mugmL(-1) (propylparaben) and recovery from the pharmaceutical preparations in the range 97.50-98.94%. The chromatographic resolution between peaks of compounds was more than 4.5 and analysis time was 5.1min under the optimal conditions. The advantages of sequential injection chromatography against classical HPLC are discussed and showing that SIC can be a method of option in many cases." @default.
- W2067219679 created "2016-06-24" @default.
- W2067219679 creator A5023836074 @default.
- W2067219679 creator A5033866908 @default.
- W2067219679 creator A5054297242 @default.
- W2067219679 creator A5089113336 @default.
- W2067219679 date "2007-04-01" @default.
- W2067219679 modified "2023-09-24" @default.
- W2067219679 title "A novel application of Onyx™ monolithic column for simultaneous determination of salicylic acid and triamcinolone acetonide by sequential injection chromatography" @default.
- W2067219679 cites W1975008964 @default.
- W2067219679 cites W1977875987 @default.
- W2067219679 cites W1978472667 @default.
- W2067219679 cites W2003056190 @default.
- W2067219679 cites W2009109454 @default.
- W2067219679 cites W2009232111 @default.
- W2067219679 cites W2027545007 @default.
- W2067219679 cites W2030073021 @default.
- W2067219679 cites W2032663569 @default.
- W2067219679 cites W2034019771 @default.
- W2067219679 cites W2053020076 @default.
- W2067219679 cites W2064123588 @default.
- W2067219679 cites W2065163270 @default.
- W2067219679 cites W2079440572 @default.
- W2067219679 cites W2092900416 @default.
- W2067219679 cites W2095391510 @default.
- W2067219679 cites W2106989592 @default.
- W2067219679 cites W2130004951 @default.
- W2067219679 cites W4230661041 @default.
- W2067219679 doi "https://doi.org/10.1016/j.talanta.2006.12.009" @default.
- W2067219679 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/19071698" @default.
- W2067219679 hasPublicationYear "2007" @default.
- W2067219679 type Work @default.
- W2067219679 sameAs 2067219679 @default.
- W2067219679 citedByCount "32" @default.
- W2067219679 countsByYear W20672196792012 @default.
- W2067219679 countsByYear W20672196792013 @default.
- W2067219679 countsByYear W20672196792015 @default.
- W2067219679 countsByYear W20672196792017 @default.
- W2067219679 countsByYear W20672196792019 @default.
- W2067219679 countsByYear W20672196792020 @default.
- W2067219679 countsByYear W20672196792023 @default.
- W2067219679 crossrefType "journal-article" @default.
- W2067219679 hasAuthorship W2067219679A5023836074 @default.
- W2067219679 hasAuthorship W2067219679A5033866908 @default.
- W2067219679 hasAuthorship W2067219679A5054297242 @default.
- W2067219679 hasAuthorship W2067219679A5089113336 @default.
- W2067219679 hasConcept C113196181 @default.
- W2067219679 hasConcept C119128265 @default.
- W2067219679 hasConcept C141071460 @default.
- W2067219679 hasConcept C178790620 @default.
- W2067219679 hasConcept C179998833 @default.
- W2067219679 hasConcept C185592680 @default.
- W2067219679 hasConcept C2777415180 @default.
- W2067219679 hasConcept C2777463227 @default.
- W2067219679 hasConcept C2778221352 @default.
- W2067219679 hasConcept C2778903070 @default.
- W2067219679 hasConcept C2781087243 @default.
- W2067219679 hasConcept C43617362 @default.
- W2067219679 hasConcept C55493867 @default.
- W2067219679 hasConcept C67031304 @default.
- W2067219679 hasConcept C71924100 @default.
- W2067219679 hasConceptScore W2067219679C113196181 @default.
- W2067219679 hasConceptScore W2067219679C119128265 @default.
- W2067219679 hasConceptScore W2067219679C141071460 @default.
- W2067219679 hasConceptScore W2067219679C178790620 @default.
- W2067219679 hasConceptScore W2067219679C179998833 @default.
- W2067219679 hasConceptScore W2067219679C185592680 @default.
- W2067219679 hasConceptScore W2067219679C2777415180 @default.
- W2067219679 hasConceptScore W2067219679C2777463227 @default.
- W2067219679 hasConceptScore W2067219679C2778221352 @default.
- W2067219679 hasConceptScore W2067219679C2778903070 @default.
- W2067219679 hasConceptScore W2067219679C2781087243 @default.
- W2067219679 hasConceptScore W2067219679C43617362 @default.
- W2067219679 hasConceptScore W2067219679C55493867 @default.
- W2067219679 hasConceptScore W2067219679C67031304 @default.
- W2067219679 hasConceptScore W2067219679C71924100 @default.
- W2067219679 hasFunder F4320321005 @default.
- W2067219679 hasIssue "2" @default.
- W2067219679 hasLocation W20672196791 @default.
- W2067219679 hasLocation W20672196792 @default.
- W2067219679 hasOpenAccess W2067219679 @default.
- W2067219679 hasPrimaryLocation W20672196791 @default.
- W2067219679 hasRelatedWork W1603333022 @default.
- W2067219679 hasRelatedWork W1964259887 @default.
- W2067219679 hasRelatedWork W1998279148 @default.
- W2067219679 hasRelatedWork W1998842338 @default.
- W2067219679 hasRelatedWork W2013299392 @default.
- W2067219679 hasRelatedWork W2032191029 @default.
- W2067219679 hasRelatedWork W2083219894 @default.
- W2067219679 hasRelatedWork W2084062459 @default.
- W2067219679 hasRelatedWork W2096641431 @default.
- W2067219679 hasRelatedWork W2155596957 @default.
- W2067219679 hasVolume "72" @default.
- W2067219679 isParatext "false" @default.
- W2067219679 isRetracted "false" @default.
- W2067219679 magId "2067219679" @default.
- W2067219679 workType "article" @default.