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- W2067471808 abstract "When the hydrobromide adduct of di-t-butylcyclobutylmethylphosphine, P(t-Bu)2(CH2CHCH2CH2CH2) · Hbr is combined with K[PtCl3(C2H4)] and LiBr in ethanol and heated at reflux for 5 h, the σ-cyclobutyl complex forms. The complex also forms from in boiling ethanol. The structure of was deduced from spectroscopic and analytical data and confirmed by X-ray analysis of a single crystal. The complex crystallizes in the tetragonal system in space group C124ν-I41cd (a = b = 19.658(7) A, c - 15.805(6) A, A = 113 K) with 8 molecules per unit cell. The final agreement index for R(F2) is 0.075 for the 2403 unique data (including F02 < 0). Bond lengths in the five-membered chelate ring PtPC(3)C(10)C(11) are PtP 2.198(4), PC(3) 1.875(18). C(3)C(10) 1.53(2), C(10)C(11) 1.57(2), C(11)Pt 2.079(17) A. The remaining cyclobutyl bond distances are C(11)C(12) 1.56(2), C(12)C(13) 1.51(3), C(10)C(13) 1.53(3) A. The PtBr bond distances are 2.510(2) and 2.612(2) A for bromine cis- and trans- to atom C(11), respectively." @default.
- W2067471808 created "2016-06-24" @default.
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- W2067471808 date "1987-08-01" @default.
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- W2067471808 title "Formation of a σ-cyclobutyl-platinum bond by the intramolecular activation of a cyclobutylphosphine. Synthesis and structure of" @default.
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- W2067471808 doi "https://doi.org/10.1016/0022-328x(87)80294-2" @default.
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