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• W2067793566 abstract "Abstract An efficient diversity‐oriented procedure for the two‐step synthesis of 3‐benzazepines is described. The Cu I ‐catalyzed three‐component coupling of an aldehyde, an alkyne and an amine (A 3 ‐coupling) provides the required propargylamines and assures the generation of diversity. The Pd‐catalyzed intramolecular acetylene hydroarylation reaction selectively creates the seven‐membered 3‐benzazepine framework with full control over the ring size and the geometry around the double bond. Microwave irradiation is demonstrated to be highly efficient in promoting both steps." @default.
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• W2067793566 date "2010-07-16" @default.
• W2067793566 modified "2023-10-07" @default.
• W2067793566 title "Diversity‐Oriented Microwave‐Assisted Synthesis of the 3‐Benzazepine Framework" @default.
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• W2067793566 doi "https://doi.org/10.1002/ejoc.201000583" @default.
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