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• W2068023907 abstract "The commercial hyperbranched aliphatic polyols (Hn) were modified by thioglycolic acid (TA) and hexafluorobutyl acrylate (HFBA) or dodecafluoroheptyl methacrylate (DFHMA) to prepare a series of fluorinated hyperbranched polyesters. For comparison, a linear fluorinated polymer, poly(n-BMA-co-DFHMA), was synthesized through the copolymerization of n-butyl methacrylate (BMA) and DFHMA. The molecular structures were characterized by 1H NMR spectroscopic analysis. The synthesized polymers were incorporated into UV-curable formulations as additives, and exposed to a UV lamp. After UV curing, the wettability of the films was investigated by contact angle measurement with water and 1-bromonaphthalene. The results showed that both the hydrophobicity and oleophobicity were greatly enhanced. Moreover, the fluorinated hyperbranched polymers possessed better water and oil repellency than the copolymer poly(n-BMA-co-DFHMA) at a very low concentration. The surface F/C ratio values of the cured films were detected by XPS analysis, and the film with TAH20–DFHMA showed the highest F/C ratio value, indicating its most efficient aggregation effect at the film surface." @default.
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• W2068023907 date "2010-12-01" @default.
• W2068023907 modified "2023-10-16" @default.
• W2068023907 title "Fluorinated modification of hyperbranched polyesters used for improving the surface property of UV curing coatings" @default.
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• W2068023907 doi "https://doi.org/10.1016/j.jfluchem.2010.09.008" @default.
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