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- W2068193622 abstract "Abstract The distribution of X-ray radiation from a small particle, situated near the sharp edge of a flat substrate and excited by an electron beam, is analyzed theoretically taking into account the effects of the radiation reflection and its partial penetration through the substrate lateral surface. It has been shown that in some cases this dependence is strongly related to the distribution of primary X-ray sources above the substrate, which allows to use the signal — grazing-angle dependence for structure investigations of particles. The proposed technique was tested in experiments with CaCO 3 particles, situated on a pure Si substrate and exposed to a highly concentrated HNO 3 environment. Comparison of the observed angle dependencies for Ca and O characteristic X-ray radiation with calculated results revealed the intrinsic structure of the particles caused by their preliminary chemical treatment." @default.
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- W2068193622 date "2001-12-01" @default.
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- W2068193622 title "Grazing-emission electron probe microanalysis of particles near the substrate edge" @default.
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- W2068193622 doi "https://doi.org/10.1016/s0584-8547(01)00300-7" @default.
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