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- W2068239787 abstract "The chelating organic ligands of 2,2′-bipyridine (2,2′-bipy), di(pyrid-2-yl)amine (dpa) and 2,6-di(pyrid-2-ylamino)pyridine (dpap) were respectively applied to react with H2fum (fumaric acid) and copper salts, affording three different complexes [Cu2(fum)(2,2′-bipy)4]·2ClO4 (1), [Cu2(µ-OH)2(fum)(dpa)2]·2H2O (2) and [Cu(SO4)(H2O)(dpap)]·H2O (3). These complexes were determined by single-crystal X-ray diffraction. Each penta-coordinated Cu(II) ion exhibits a distorted trigonal bipyramidal geometry in 1. The fum ligand links copper ions to form a dinuclear copper unit. While in 2, the fum ligands connect [Cu2(µ-OH)2(dpa)2] unit to construct a 1D zigzag chain. Unexpectedly, when dpap instead of dpa was used under the same conditions, only one mononuclear complex 3 was formed. Crystal packings show that 1–3 form 3D supramolecular architectures through non-covalent interactions (multiple hydrogen bonds and C–H··· π/π-π interactions). In addition, the study of the magnetic property reveals dominating ferromagnetic interactions between Cu(II) atoms in 1." @default.
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- W2068239787 date "2009-02-01" @default.
- W2068239787 modified "2023-09-27" @default.
- W2068239787 title "Synthesis and Characterization of Three Diverse Coordination Frameworks under Co-ligand Intervention" @default.
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- W2068239787 doi "https://doi.org/10.1002/cjoc.200990051" @default.
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