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- W2068273497 abstract "14C-Anthranilic acid has been prepared in a fast and efficient way in a two-step reaction in 82% overall radiochemical yield. Thus, 2-iodoaniline was transformed into 2-amino-[7-14C]-benzonitrile using a palladium catalyzed cyanation with zinc 14C-cyanide. Subsequent basic hydrolysis of the cyano group afforded [7-14C]-anthranilic acid. The method was successfully applied to a benzophenone scaffold, 4-iodophenol and 4-iodobenzoic acid producing the corresponding carboxylic acids in good to excellent radiochemical yields (62–82%) and with high specific activity (1.94–1.98 GBq/mmol). Copyright © 2009 John Wiley & Sons, Ltd." @default.
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- W2068273497 date "2009-05-15" @default.
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- W2068273497 title "Fast and efficient synthesis of<sup>14</sup>C labelled benzonitriles and their corresponding acids" @default.
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- W2068273497 doi "https://doi.org/10.1002/jlcr.1585" @default.
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