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W2068417892 abstract "Using the TiCl3H2O2 radical-generating method at 10–40°C, we have successfully characterized by EPR radicals formed from the substrates ulbarcyclopentanone, I, and methyl 2-oxocyclopentanecarboxylate, II; , 1, and , 2, and, from II, , 3. The spectrum of 1 was particularly interesting as it displayed higher-order effects arising from the interaction of two pairs of nearly equivalent β-CH2 protons (each member of a pair at the same carbon being equivalent). The previous EPR investigators of this radical did not notice this effect. The results for 2 were in reasonable agreement with the literature and those for the hitherto unreported 3 were in line with expectation. To assist with splitting-constant assignments and conformational analyses we utilized INDO-MO-SCF calculations in the case of 1 and 2 and splitting-constant temperature dependency studies for 3." @default.
W2068417892 created "2016-06-24" @default.
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W2068417892 date "1988-08-01" @default.
W2068417892 modified "2023-09-27" @default.
W2068417892 title "EPR study of radicals derived from cyclopentanone and methyl 2-oxocyclopentanecarboxylate" @default.
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W2068417892 doi "https://doi.org/10.1016/0022-2364(88)90327-7" @default.
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