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- W2068432453 abstract "Spinel lithium manganese oxide was synthesized via co-precipitation. The prepared lithium manganese oxide powder was further heated at 700 ◦ C for 15 h under pressurized (3 bar) oxygen atmosphere. The resultant exhibited a highly crystalline cubic spinel phase with space group Fd3m, as confirmed by X-ray diffraction. The spinel compound exhibited a slightly smaller lattice constant than a conventional spinel compound, even though the cationic ratio of Li/Mn is the same for both compounds. Chemical titration of the Mn component showed that heat treatment under a 3 bar oxygen atmosphere resulted in slightly higher average Mn oxidation state, indicating that the amount of Mn4+ increased after the treatment. The Li1.05Mn1.95O3.99 electrode exhibited improved cycling performance, namely, 96.3% of capacity retention during 100 cycles at elevated temperature (60 ◦ C). The details of the structure and electrochemistry of the electrode are discussed." @default.
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- W2068432453 date "2010-12-01" @default.
- W2068432453 modified "2023-10-14" @default.
- W2068432453 title "Spinel lithium manganese oxide synthesized under a pressurized oxygen atmosphere" @default.
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- W2068432453 doi "https://doi.org/10.1016/j.electacta.2010.07.051" @default.
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