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- W2068443886 abstract "Abstract Reaction of H2Os3(CO)10 with PhCCBr produced a vinyltriosmium complex Os3(CO)10(μ-Br)(CHCHPh) (1) in high yield. Thermolysis of complex 1 in refluxing toluene produced a hydrido-vinylidene complex Os3(CO)9(μ-H)(μ-Br)(CCHPh) (2); the crystal structure and reactivity of complexes 1 and 2 have been studied. Crystal data for complex 1: space group P 2 1 c , a 14.049(6), b 10.035(4), c 15.933(6) A, β 93.06(4)°, Z = 4; RF 6.32%, Rw 6.33%, GOF = 1.49. Crystal data for complex 2: space group P 1 n ,a 14.047(4), b 10.439(3), c 15.636(4) A, β 114.28(3)°, Z = 4; RF 3.80%, Rw 4.38%, GOF = 0.73." @default.
- W2068443886 created "2016-06-24" @default.
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- W2068443886 date "1989-11-01" @default.
- W2068443886 modified "2023-09-27" @default.
- W2068443886 title "Synthesis, structure and reactivity studies of triosmium complexes, Os3(CO)10(μ-Br)(CHCHPh) and Os3(CO)9(μ-H)(μ-Br)(CCHPh)" @default.
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- W2068443886 doi "https://doi.org/10.1016/0022-328x(89)80103-2" @default.
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