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• W2068447430 endingPage "8689" @default.
• W2068447430 startingPage "8684" @default.
• W2068447430 abstract "Synthetic mineral libethenite Cu2PO4OH was prepared by the hydrothermal method, and its structure at 200 K was refined by single-crystal X-ray diffraction. The structure of Cu2PO4OH is built up from Cu22O6(OH)2 dimers of edge-sharing Cu2O4(OH) trigonal bipyramids and [Cu12O6(OH)2]∝ chains of edge-sharing Cu1O4(OH)2 octahedra. Magnetic properties of Cu2PO4OH were investigated by magnetic susceptibility, magnetization, and specific heat measurements. Cu2PO4OH is a spin-gap system with a spin gap of about 139 K. It was shown by spin dimer analysis that, to a first approximation, the magnetic structure of Cu2PO4OH is described by an isolated square-spin cluster model defined by the Cu1−O−Cu2 superexchange J with Cu1···Cu2 = 3.429 Å. The fitting analysis of the magnetic susceptibility data with a square-spin cluster model results in J/kB = 138 K. Specific heat data show that Cu2PO4OH does not undergo a long-range magnetic ordering down to 1.8 K. We also report vibrational properties studied with Raman spectroscopy and the thermal stability of Cu2PO4OH." @default.
• W2068447430 created "2016-06-24" @default.
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• W2068447430 date "2007-09-12" @default.
• W2068447430 modified "2023-10-13" @default.
• W2068447430 title "Magnetic Properties of Synthetic Libethenite Cu₂PO₄OH: a New Spin-Gap System" @default.
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• W2068447430 doi "https://doi.org/10.1021/ic7008418" @default.
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