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• W2068473081 abstract "Radiation-induced decomposition of the anion exchange resin Amberlite IRA-400 in hydroxide form by gamma radiolysis has been studied under different irradiation doses and irradiation atmospheres. In this work, we focused on the degradation of the solid part of the resin by Fourier transformed infrared (FTIR) and 13C nuclear magnetic resonance (NMR) spectroscopies associated with chemometric treatments. FTIR and 13C NMR techniques showed that only CH2N+(CH3)3 groups were detached from the resin whereas the polystyrene divinylbenzene backbone remains intact. The quaternary ammonium groups were replaced by amine or carbonyl groups according to the irradiation atmosphere (with or without water or oxygen). Principal components analysis (PCA) was used to classify the degraded resins according to their irradiation conditions by separating the effect of the dose or the environment. The PCA loadings have shown spectral regions which discriminate the irradiated resins whereas SIMPLe-to-use Interactive Self-modeling Mixture Analysis (SIMPLISMA) allows to identify families of component characterizing the chemical structure of resins and estimate their relative contributions according to the irradiation atmospheres." @default.
• W2068473081 created "2016-06-24" @default.
• W2068473081 creator A5019390482 @default.
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• W2068473081 creator A5059113897 @default.
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• W2068473081 date "2012-03-01" @default.
• W2068473081 modified "2023-09-25" @default.
• W2068473081 title "Investigation of gamma radiation effect on the anion exchange resin Amberlite IRA-400 in hydroxide form by Fourier transformed infrared and 13C nuclear magnetic resonance spectroscopies" @default.
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• W2068473081 doi "https://doi.org/10.1016/j.aca.2011.12.046" @default.
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• W2068473081 hasPublicationYear "2012" @default.
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